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162�C164?��C; 1H NMR (400?MHz, CDCl3) ��: 3.Eighty eight (3H, azines), 3.96 Oxygenase (3H, azines), 7.02 (2H, m), 7.31 (1H, dd, J=8.8?Hz, J=2.8?Hz), 7.Forty one (1H, ersus), 7.62 (1H, n, J=8.8?Hz), 7.Sixty nine (2H, Hydroxychloroquine mouse m), 8.50 (1H, n, J=2.8?Hz); Microsoft (ESI+) m/z: 299.1 [M+H]+. HR-MS (ESI+) m/z: 299.0745 [M+H]+, Calcd. with regard to C17H15O3S 299.0736. 6-Methoxy-2-methyl-4H-thiochromen-4-one (7e): yield 60%, mp. 100�C102?��C; 1H NMR (400?MHz, DMSO-d6) ��: 2.Forty-nine (3H, ersus), 3.Ninety three (3H, ersus), 6.Ninety two (1H, ersus), 7.12 (1H, dd, J=3.2 Hertz, J=8.8?Hz), 7.Forty-eight (1H, n, J=8.8?Hz), 7.Ninety-six (1H, deborah, J=3.2?Hz); Microsoft (ESI+) m/z: 207.2 [M+H]+, 229.2 [M+Na]+; HR-MS (ESI+) m/z: 207.0479 [M+H]+, Calcd. for C11H11O2S 207.0474. 2-(Chloromethyl)-6-methoxy-4H-thiochromen-4-one (7f): produce 40%, mega pixel. 129�C132?��C; 1H NMR (400?MHz, DMSO-d6) ��: 3.Eighty-eight (3H, ersus), 4.89 (2H, s), 7.Twelve (1H, utes), 7.Forty-one (1H, dd, J=2.8?Hz, J=8.8?Hz), 7.Seventy six (1H, d, J=2.8?Hz), 7.87 (1H, d, J=8.8?Hz); MS (ESI+) m/z: 241.2 [M+H]+, More than 200.2 [M+Na]+; HR-MS (ESI+) m/z: 241.0082 [M+H]+, Calcd. regarding C11H10ClO2S 241.0090. 6-Methoxy-2-methyl-3-phenyl-4H-thiochromen-4-one (7g): produce 58%, mp. 107�C109?��C; 1H NMR (400?MHz, DMSO-d6) ��: 2.21 years of age (3H, s), 3.Ninety (3H, s), 7.16 (2H, n, J=6.8?Hz,), 7.Forty five (3H, michael), 7.Thirty-eight (1H, dd, J=2.8?Hz, J=8.8?Hz), 7.Seventy six (1H, deborah, J=2.8?Hz), 7.Seventy nine (1H, d, J=8.8?Hz); Microsof company (ESI+) m/z: 283.5 [M+H]+, 305.3 [M+Na]+. HR-MS (ESI+) m/z: 283.0795 [M+H]+, Calcd. with regard to C17H15O2S 283.0787. 6-Methoxy-2-(4-nitrophenyl)-4H-thiochromen-4-one (7h): generate 45%, megapixel. 186�C188?��C; Fasudil cell line 1H NMR (400?MHz, DMSO-d6) ��: 3.91 (3H, s), 7.22 (1H, utes), 7.46 (1H, dd, J=2.8?Hz, J=8.8?Hz), 7.Eighty three (1H, d, J=2.8?Hz), 7.Ninety five (1H, d, J=8.8?Hz), 8.04 (2H, deborah, J=8.8?Hz), 8.Forty-four (2H, d, J=8.8?Hz); Microsoft (ESI+) m/z: 314.2 [M+H]+; HR-MS (ESI+) m/z: 314.0491 [M+H]+, Calcd. regarding C16H12O4NS 314.0482. 3-Chloro-6-methoxy-2-methyl-4H-thiochromen-4-one (7i): yield: 40%, megapixel. 90�C93?��C; 1H NMR (400?MHz, DMSO-d6) ��: 2.50 (3H, azines), 3.Ninety (3H, utes), 7.35 (1H, dd, J=2.8?Hz, J=8.8?Hz), 7.76 (1H, deborah, J=2.8?Hz), 7.77 (1H, d, J=8.8?Hz); HR-MS(ESI+) m/z: 241.0091 [M+H]+, Calcd.
